Experimental Characterization of Milling, Compaction and Sintering of Nanocrystalline FC-0205 Copper Steel Powder

Jamel H. Alexander; Olalekan R. Junaid; Tonya W. Stone

Experimental Characterization of Milling, Compaction and Sintering of Nanocrystalline FC-0205 Copper Steel Powder

Jamel H. Alexander * §

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Olalekan R. Junaid

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Tonya W. Stone

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§ Mississippi State University

Experimental Characterization of Milling, Compaction and Sintering of Nanocrystalline FC-0205 Copper Steel Powder

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Abstract

The effect of ball milling on the compaction and sintering of nanocrystalline copper steel powder (FC-0205) was evaluated within this work. The as-received micron-sized FC-0205 copper steel powder was subjected to High Energy Ball Milling (HEBM) in an argon atmosphere at different milling times of 0, 16, 20 and 24 hours to obtain nanocrystalline structures. Unmilled, 8 and 16 hours milled powders were compacted using uniaxial die compression at pressures ranging from 274 MPa to 775 MPa to obtain a relative density range of 74% to 95%, respectively. The steel powder compacts were sintered at temperatures ranging from 400 °C to 1120 °C in high purity hydrogen and nitrogen atmospheres. X-ray Diffraction (XRD) and microscopy analysis were performed on the milled powder specimens to evaluate particle size, morphology, and extent of porosity; to establish a relationship between milling time and particle size, and to establish a correlation between grain size and milling time.

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Funding

No external funding was declared for this work.

Conflict of Interest

The authors declare no conflict of interest.

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No ethics committee approval was required for this article type.

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How to Cite This Article

Jamel H. Alexander, Olalekan R. Junaid, Tonya W. Stone. 2018. "Experimental Characterization of Milling, Compaction and Sintering of Nanocrystalline FC-0205 Copper Steel Powder". Global Journal of Research in Engineering - A : Mechanical & Mechanics GJRE-A Volume 18 (GJRE Volume 18 Issue A1).

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GJRE Volume 18 Issue A1

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Journal Specifications

Crossref Journal DOI 10.17406/gjre

Print ISSN 0975-5861

e-ISSN 2249-4596

Keywords

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Classification

GJRE-A Classification FOR Code: 091399

Submission ReceivedDecember 7, 2017
Peer Review Double Blind
Handling Editor
Accepted January 3, 2018
Published January 15, 2018

Version of record

v1.2

Issue date

June 26, 2018

Language

English

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Article Matrices

Total Score: 133

Country: United States

Subject: Global Journal of Research in Engineering

Authors: Olalekan R. Junaid, Tonya W. Stone, Jamel H. Alexander (PhD/Dr. count: 0)

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