Chemistry Synthesis, Characterization and Photocatalysis of KSr2Nb5O15 doped with Nickel

Article ID

X034Y

Chemistry Synthesis, Characterization and Photocatalysis of KSr2Nb5O15 doped with Nickel

Paulo Cesar Faria
Paulo Cesar Faria University of the State of Sao Paulo
DOI

Abstract

Potassium and strontium niobate (KSr2Nb5O15) of tungsten structure (TB) bronze was doped with nickel (Ni2+) with stoichiometry type KSr2NixNb5-xO15-δ onde x = 0,25; 0,50 and 0,75. The powders were prepared by chemical synthesis using the modified Polyol method, and characterized by infrared spectroscopy with Fourier transform (FT-IR), by X-ray diffraction (XRD), including the network parameters (relative intensity – IR(KSNNi0,50) ˃ IR(KSNNI0,25) ˃ IR(KSNNI0,75) ) and crystallite size. The effects of doping (Ni2+) in the process of photo degradation were studied, the absorbance as a function of time for the Basic Blue dye 41 result from the photo degradation performed with the photo catalyst KSNNi0,50 presented a lower absorbance value, and the spectrophotometer was used in the UV-vis region.

Chemistry Synthesis, Characterization and Photocatalysis of KSr2Nb5O15 doped with Nickel

Potassium and strontium niobate (KSr2Nb5O15) of tungsten structure (TB) bronze was doped with nickel (Ni2+) with stoichiometry type KSr2NixNb5-xO15-δ onde x = 0,25; 0,50 and 0,75. The powders were prepared by chemical synthesis using the modified Polyol method, and characterized by infrared spectroscopy with Fourier transform (FT-IR), by X-ray diffraction (XRD), including the network parameters (relative intensity – IR(KSNNi0,50) ˃ IR(KSNNI0,25) ˃ IR(KSNNI0,75) ) and crystallite size. The effects of doping (Ni2+) in the process of photo degradation were studied, the absorbance as a function of time for the Basic Blue dye 41 result from the photo degradation performed with the photo catalyst KSNNi0,50 presented a lower absorbance value, and the spectrophotometer was used in the UV-vis region.

Paulo Cesar Faria
Paulo Cesar Faria University of the State of Sao Paulo

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Paulo Cesar Faria. 2019. “. Global Journal of Research in Engineering – C: Chemical Engineering GJRE-C Volume 19 (GJRE Volume 19 Issue C2): .

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Crossref Journal DOI 10.17406/gjre

Print ISSN 0975-5861

e-ISSN 2249-4596

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GJRE-C Classification: FOR Code: 290601
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Chemistry Synthesis, Characterization and Photocatalysis of KSr2Nb5O15 doped with Nickel

Paulo Cesar Faria
Paulo Cesar Faria University of the State of Sao Paulo

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