Synthesis and Research of New Compounds of Guanidine on the Basis of α-Chlorether and Chlorazone

Synthesis and Research of New Compounds of Guanidine on the Basis of α-Chlorether and Chlorazone

S.R.Hajiyeva

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G.I.Bayramov

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F.Е.Huseynov

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T.I.Aliyeva

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H.L.Rafiyeva

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Z.T.Valiyeva

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A.A.Samadova

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N.M.Jafarova

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Baku State University

Synthesis and Research of New Compounds of Guanidine on the Basis of α-Chlorether and Chlorazone

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Abstract

The reactions of chlorazone with α-chloroethyl esters of n-C 8 H 17 OH, n-C 10 H 21 OH, n-C 12 H 25 OH, CH 3 -CH=CCl-CH 2 OH alcohols for the first time were carried out, and chlorazone esters containing two ROCH 2 groups of these esters were obtained. The reactions of N 1 -alkoxymethyl-N 3 -alkoxymethylguanidine compounds with these chlorazone esters were carried out and 4 new guanidine derivatives (conventionally designated as I-IV) were synthesized, not known in the literature. Studies have been conducted to establish corrosion inhibitory efficiency for each of the newly synthesized compounds of guanidine I-IV in a very strong aggressive environment created in the laboratory. It was established that the inhibitory effectiveness of these compounds in concentrations of 1.0; 2.0; 2.5 mg/l is 99.97-100%. A comparative study of the effective inhibitory properties of the new synthesized guanidine compounds for corrosion protection of steel “St.3” was carried out. Studies have shown that each of the new I-IV compounds of guanidine in terms of environmental safety, economic and environmental efficiency is 5-10 times higher than the inhibitors currently used to protect from corrosion steel processing equipment operating in aggressive environments.

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Funding

No external funding was declared for this work.

Conflict of Interest

The authors declare no conflict of interest.

Ethical Approval

No ethics committee approval was required for this article type.

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Not applicable for this article.

How to Cite This Article

S.R.Hajiyeva. 2020. \u201cSynthesis and Research of New Compounds of Guanidine on the Basis of α-Chlorether and Chlorazone\u201d. Global Journal of Science Frontier Research - B: Chemistry GJSFR-B Volume 20 (GJSFR Volume 20 Issue B2).

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GJSFR Volume 20 Issue B2

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Journal Specifications

Crossref Journal DOI 10.17406/GJSFR

Print ISSN 0975-5896

e-ISSN 2249-4626

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GJSFR-B Classification FOR Code: 250399

Submission ReceivedMarch 5, 2020
Peer Review Double Blind
Handling Editor
Accepted March 30, 2020
Published April 10, 2020

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v1.2

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September 8, 2020

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