Qualitative and Quantitative Analysis for Determination of Glue Snifferas Urine

Qualitative and Quantitative Analysis for Determination of Glue Snifferas Urine

Mohamad Raizul Zinalibdin Master of Science (Chemistry)

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Abdul Rahim Yacob

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α University of Technology Malaysia

Qualitative and Quantitative Analysis for Determination of Glue Snifferas Urine

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Abstract

Inhalant abuse is defined as an intentional inhalation of solvents or volatile substances present in materials such as glues and paints. The most commonly abused inhalant today is glue due to low price and easy access. Glue sniffing produces fast and pleasurable sensory experience to the abuser. Quantitative analysis of hippuric acid using UV-Vis at wavelength 417 nm was determined successfully. The results gave a regression coefficient of 0.994. The recovery, accuracy and coefficient variance of hippuric acid were 96.57%, 2.94% and 0.50% respectively. Reversed-phase high performance liquid chromatography using a simple method for the simultaneous determination of hippuric acid and benzoic acid was also described. The chromatography was performed on a Nova-Pak C18 (3.9 x 150 mm) column with a mobile phase of methanol: water: acetic acid (20:80:0.2) using UV detection at 254 nm. The calibration of standards was linear within concentration range of 0.125 to 6.0 mg/mL of hippuric acid and benzoic acid respectively.

References

14 Cites in Article

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Funding

No external funding was declared for this work.

Conflict of Interest

The authors declare no conflict of interest.

Ethical Approval

No ethics committee approval was required for this article type.

Data Availability

Not applicable for this article.

How to Cite This Article

Mohamad Raizul Zinalibdin. 2014. \u201cQualitative and Quantitative Analysis for Determination of Glue Snifferas Urine\u201d. Global Journal of Science Frontier Research - B: Chemistry GJSFR-B Volume 14 (GJSFR Volume 14 Issue B3): .

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GJSFR Volume 14 Issue B3
Pg. 23- 28

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Journal Specifications

Crossref Journal DOI 10.17406/GJSFR

Print ISSN 0975-5896

e-ISSN 2249-4626

Keywords

glue hippuric acid ultra violet-visible

Submission ReceivedMay 3, 2014
Peer Review Double Blind
Handling Editor
Accepted May 31, 2014
Published June 11, 2014

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v1.2

Issue date

June 21, 2014

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Article Matrices

Total Score: 102

Country: Unknown

Subject: Global Journal of Science Frontier Research - B: Chemistry

Authors: Abdul Rahim Yacob, Mohamad Raizul Zinalibdin (PhD/Dr. count: 0)

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Total Views: 4527

Total Downloads: 2333

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