Synthesis and Spectral Characterization Of Thorium (IV) Complexes With 3-Substituted-4-Amino-5-Mercapto-1,2,4-Triazole Schiff Bases

Synthesis and Spectral Characterization Of Thorium (IV) Complexes With 3-Substituted-4-Amino-5-Mercapto-1,2,4-Triazole Schiff Bases

Dr. Mallikarjun S Yadawe M.Sc., Ph.D.

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Sangamesh A Patil

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α Rani Channamma University, Belagavi

Synthesis and Spectral Characterization Of Thorium (IV) Complexes With 3-Substituted-4-Amino-5-Mercapto-1,2,4-Triazole Schiff Bases

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Synthesis and Spectral Characterization Of Thorium (IV) Complexes With 3-Substituted-4-Amino-5-Mercapto-1,2,4-Triazole Schiff Bases Banner

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Abstract

complexes have been synthesized by reacting Th(IV) nitrate with Schiff bases derived from 3-substituted-4-amino-5-mercapto-1,2,4-triazole and glyoxal/ biacetyl/ benzyl in ethanol. These complexes have been characterized on the basis of elemental analysis, molar conductance and spectral studies. Analytical and spectral data suggest structures in which Th(IV) is six coordinated. All these complexes are light yellow in colour and are insoluble in DMF and DMSO. The elemental analysis show that, the complexes analysed for 1:1 stoichiometry of the type, Th.LH 2 (NO 3 ) 4 .Conductance measurement in DMF are too low to account for any dissociation of these complexes in DMF at the concentration of the 10 -3 M.

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Funding

No external funding was declared for this work.

Conflict of Interest

The authors declare no conflict of interest.

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No ethics committee approval was required for this article type.

Data Availability

Not applicable for this article.

How to Cite This Article

Dr. Mallikarjun S Yadawe. 2012. \u201cSynthesis and Spectral Characterization Of Thorium (IV) Complexes With 3-Substituted-4-Amino-5-Mercapto-1,2,4-Triazole Schiff Bases\u201d. Global Journal of Science Frontier Research - B: Chemistry GJSFR-B Volume 12 (GJSFR Volume 12 Issue B5): .

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GJSFR Volume 12 Issue B5
Pg. 41- 44

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Journal Specifications

Crossref Journal DOI 10.17406/GJSFR

Print ISSN 0975-5896

e-ISSN 2249-4626

Keywords

elemental analysis Synthesis Th(IV) complexes

Submission ReceivedAugust 13, 2012
Peer Review Double Blind
Handling Editor
Accepted September 10, 2012
Published September 25, 2012

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October 2, 2012

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Total Score: 107

Country: Unknown

Subject: Global Journal of Science Frontier Research - B: Chemistry

Authors: Dr. Mallikarjun S Yadawe, Sangamesh A Patil (PhD/Dr. count: 1)

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