Synthesis, Spectroscopic, Thermodynamic and Biological Activity Studies of Schiff Base and Metal Complexes Derived From 2-[ 1H-Pyrrol-2-Ylimino Methyl]- 5-Phenyl-1,3,4- Oxadiazole

Article ID

TJ13U

Synthesis, Spectroscopic, Thermodynamic and Biological Activity Studies of Schiff Base and Metal Complexes Derived From 2-[ 1H-Pyrrol-2-Ylimino Methyl]- 5-Phenyl-1,3,4- Oxadiazole

Nazk Mohammed Aziz
Nazk Mohammed Aziz University of Sulaimani
Naser Dhiya Shaalan
Naser Dhiya Shaalan
DOI

Abstract

New metal complexes of the ligand (HL) 2-[1H-Pyrrol-2-ylimino methyl]- 5-phenyl-1, 3,4-oxadiazol with the metal ions Co(II), Ni(II) and Cu(II), were prepared in alcoholic medium. The Schiff bases were condensed by using [Pyrrolcarboxaldehyde] with[2-amino-5-(phenyl-1, 3,4-oxadiazole] in alcoholice medium. As the Schiff baseprepared was tridentate ligand, it was used for forming complexes with Co+2, Ni+2, Cu +2 and Zn+2 ions of type M (HL)2. All the synthesized Schiff base and their metal complexes were characterized by FTIR Spectroscopy, Electronic Spectroscopy, Elemental Analysis, Magnetic Susceptibility Measurements, Thermal Analysis , 1H-NMRSpectra, and Mass Spectra.

Synthesis, Spectroscopic, Thermodynamic and Biological Activity Studies of Schiff Base and Metal Complexes Derived From 2-[ 1H-Pyrrol-2-Ylimino Methyl]- 5-Phenyl-1,3,4- Oxadiazole

New metal complexes of the ligand (HL) 2-[1H-Pyrrol-2-ylimino methyl]- 5-phenyl-1, 3,4-oxadiazol with the metal ions Co(II), Ni(II) and Cu(II), were prepared in alcoholic medium. The Schiff bases were condensed by using [Pyrrolcarboxaldehyde] with[2-amino-5-(phenyl-1, 3,4-oxadiazole] in alcoholice medium. As the Schiff baseprepared was tridentate ligand, it was used for forming complexes with Co+2, Ni+2, Cu +2 and Zn+2 ions of type M (HL)2. All the synthesized Schiff base and their metal complexes were characterized by FTIR Spectroscopy, Electronic Spectroscopy, Elemental Analysis, Magnetic Susceptibility Measurements, Thermal Analysis , 1H-NMRSpectra, and Mass Spectra.

Nazk Mohammed Aziz
Nazk Mohammed Aziz University of Sulaimani
Naser Dhiya Shaalan
Naser Dhiya Shaalan

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Nazk Mohammed Aziz. 2015. “. Global Journal of Science Frontier Research – B: Chemistry GJSFR-B Volume 15 (GJSFR Volume 15 Issue B3): .

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Crossref Journal DOI 10.17406/GJSFR

Print ISSN 0975-5896

e-ISSN 2249-4626

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GJSFR-B Classification: FOR Code: 030306p
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Synthesis, Spectroscopic, Thermodynamic and Biological Activity Studies of Schiff Base and Metal Complexes Derived From 2-[ 1H-Pyrrol-2-Ylimino Methyl]- 5-Phenyl-1,3,4- Oxadiazole

Nazk Mohammed Aziz
Nazk Mohammed Aziz University of Sulaimani
Naser Dhiya Shaalan
Naser Dhiya Shaalan

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